Short Description
Gas adsorption according to the static-volumetric principle with six sample ports for the characterization of specific surfaces, pore systems in the nanometer range and gas-solid-body interactions in highly porous systems.
The ASAP 2420 allows for sample preparation at 12 heating ports and six simultaneous measurements for the determination of micro- and mesopore sizes, pore volumes and specific surfaces.
Contact Person
Univ.-Prof. Dr. Nicola Hüsing
Research Services
Investigations on the Structure of Nanoparticles and Mesoporous Solids
Methods & Expertise for Research Infrastructure
The gas adsorption analysis with nitrogen, argon, krypton or other gases allows the determination of specific surfaces and pore size distributions. With the ASAP2420 the physisorption isotherm of gas molecules on surfaces of porous solids can be fully determined under isothermal conditions (77 K for N2).
From the amount of adsorbed molecules as a function of the pressure p / p0, information about different models (BET, BJH, DFT, etc.), the specific surface area, pore size and size distribution, pore shape and surface properties (hydrophobic or hydrophilic) can be obtained.
At the University of Salzburg, pore and surface analyzes of porous solids or nanoparticulate solids, as powders or in monolithic form (metal powders, ceramic materials, catalysts, fillers, building materials, pigments, and many other solids) can be carried out.
Allocation to research infrastructure
Department of Molecular Biology, University of Salzburg
Various industrial partners
TU Hamburg-Harburg
Vienna University of Technology
University of Vienna
Montanuniversität Leoben
2016-2018
Musso M., Hüsing N.
Interreg Österreich-Bayern 2014-2020
http://www.interreg-bayaut.net/projekte/liste-der-vorhaben/projektzusammenfassung-tfp-hymat/
Synthese, Charakterisierung und technologische Fertigungsansätze für den Leichtbau 'n2m' (nano-to-macro)
2015-2018
Hüsing, N.; Diwald, O.; Musso, M.; Bourret, G.; Redhammer, G.; Huber, O.; Saage, H.
Interreg Österreich-Bayern 2014- 2020
http://www.interreg-bayaut.net/projekte/liste-der-vorhaben/projektzusammenfassung-ab29/
Vapor phase synthesized MgO nanocubes as seed structures in solution
2015-2016
Diwald, O.
DFG
http://gepris.dfg.de/gepris/projekt/215441693
Deformation of hierarchical and anisotropic porous solids by fluid adsorption
2014-2017
Hüsing, N.; Paris, O. (Montanuniversität Leoben), Reichenauer, G. (ZAE Bayern)
FWF, DFG
http://fodok.uni-salzburg.at/pls/portal/nav.show?x=&format=full_projekt&object=75237&lang=158
Oxidische Nanostrukturen
2013-2016
Diwald, O.
DFG
http://gepris.dfg.de/gepris/projekt/238350812
Novel Pt-poor catalysts for the electrocatalytic O2 reduction based on modified, nanostructured metal oxides
2013-2016
Hüsing N., Behm R.J.
FWF/DFG
Hybrid Supercaps
2015-2018
Hüsing, N.; Paris. O.
FFG Energieforschung/ 848808
Salzburg Center for Smart Materials
2018-2022
Hüsing, N.; Tscheligi M.; Petutschnig, A.
Europäische Union/ Land Salzburg
Salzburg Center for Smart Materials - hci.plus
Monolithic Carbon Spherogels for Electrochemical Applications
2022-2025
Elsaesser, M.S., Presser, V.
FWF/DFG
Field-Enhanced Photocatalysis at Nanoscale Gaps
2020-2024
Bourret, G.; O. Diwald
FWF
Optimizing Catalyst Loading Within Nanostructured Silicon Photoelectrodes
2020-2023
Bourret, G.; Farhadi, A.
ÖAW
Charge separation within graded metal oxide nanocomposites
2023-2026
Diwald, O.; Bourret, G.
FWF
2015
Schoiber, J.; Tippelt, G.; Redhammer, G.J.; Yada, C.; Dolotko, O.; Berger, R.J.F., Husing, N.
CRYSTAL GROWTH & DESIGN Volume: 15(9), 2015, 4213-4218.
DOI: 10.1021/acs.cgd.5b00324
Ordered Meso-/Macroporous Silica and Titania Films by Breath Figure Templating in Combination with Non-Hydrolytic Sol-Gel Processing
2015
Feinle, A.; Akbarzadeh, J.; Peterlik, H.; Hüsing, N.
Microporous and Mesoporous Materials
doi:10.1016/j.micromeso.2015.06.043
A Two-Step Synthesis for Li2CoPO4F as High-Voltage Cathode Material
2015
Schoiber, J.; Berger, R.J.F.; Yada, C.; Miki, H.; Husing, N.
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
DOI: 10.1149/2.0331514jes
Self-supporting hierarchically organized silicon networks via magnesiothermic reduction
2016
Waitzinger, M.; Elsässer, M.S.; Berger, R.J.F.; Akbarzadeh, J.; Peterlik, H.; Hüsing, N.
MONATSHEFTE FÜR CHEMIE
DOI:10.1007/s00706-015-1611-8
Sol-gel synthesis of monolithic materials with hierarchical porosity
2016
Feinle, A.; Elsässer, M.E.; Hüsing, N.
Chem. Soc. Rev.
DOI:10.1039/c5cs00710k
Chemical phase separation strategies towards silica monoliths with hierarchical porosity
2013
Triantafillidis, C.; Elsässer, M.E.; Hüsing, N.
Chem. Soc. Rev. Vol.: 42 Pages: 3833-3846
DOI:10.1039/C3CS35345A
High Surface Area Crystalline Titanium Dioxide: Potential and Limits in Electrochemical Energy Storage and Catalysis
2012
Fröschl, T.; Hörmann, U.; Kubiak, P.; Kucerova, G.; Pfanzelt, M.; Weiss, C.K.; Behm, R.J.; Hüsing, N.; Kaiser, U.; Landfester, K.; Wohlfahrt-Mehrens, M.
Chem. Soc. Rev. Vol.: 41 Pages: 5313-53,
DOI:10.1039/C2CS35013K
Reversibly compressible and freestanding monolithic carbon spherogels
2019
Miralem Salihovic, Gregor A. Zickler, Gerhard Fritz-Popovski, Maike Ulbricht, Oskar Paris, Nicola Hüsing, Volker Presser, Michael S. Elsaesser
Carbon
https://www.sciencedirect.com/science/article/pii/S0008622319306621
Monolithic Spiropyran-Based Porous Polysilsesquioxanes with Stimulus-Responsive Properties
2020
Daniel Euchler, Caroline R. Ehgartner, Nicola Hüsing, Andrea Feinle
ACS Appl. Mater. & Interf.
https://pubs.acs.org/doi/10.1021/acsami.0c14987
Monolithic Carbon Spherogels as Freestanding Electrodes for Supercapacitors
2021
Miralem Salihovic, Philipp Schlee, Servann Herou, Maria-Magdalena Titirici, Nicola Hüsing, Michael S. Elsaesser
ACS Applied Energy Materials
https://pubs.acs.org/doi/full/10.1021/acsaem.1c02055
A facile one-pot synthesis towards hierarchically organized Carbon/TiO2 monoliths with ordered mesopores
2021
Jürgen Schoiber, Christian Koczwara, Simon Rumswinkel, Laurence Whitmore, Christian Prehal, Florian. Putz, Michael S. Elsaesser, Oskar Paris, Nicola Hüsing
ChemPlusChem
https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/cplu.202000740
Renewable, Organic and Related Carbon Aerogel Monoliths from the Polycondensation of Tannin with 5-(Hydroxymethyl)furfural
2022
Ann-Kathrin Koopmann,Theresa Bartschmid, Nicola Hüsing, Michael S. Elsaesser
Journal of Sol-Gel Science and Technology
https://link.springer.com/article/10.1007/s10971-022-06015-4
Black goes green: single-step solvent exchange for sol-gel synthesis of carbon spherogels as high-performance supercapacitor electrodes
2024
Miralem Salihovic, Emmanuel Pamete´, Stefanie Arnold, Irena Sulejmani, Theresa Bartschmid, Nicola Hu¨sing, Gerhard Fritz-Popovski, Chaochao Dun, Jeffrey J. Urban, Volker Presser, M. S. Elsaesser
RSC Energy Advances
https://pubs.rsc.org/en/content/articlehtml/2024/ya/d3ya00480e
Sustainable Tannin Gels for the Efficient Removal of Metal Ions and Organic Dyes
2023
A.K. Koopmann, C.R. Ehgartner, D. Euchler, M. Claros, N. Huesing
Gels
https://doi.org/10.3390/gels9100822
Charge Separation in BaTiO3 Nanocrystals: Spontaneous Polarization Versus Point Defect Chemistry
2023
E Neige, T Schwab, M Musso, T Berger, GR Bourret, O Diwald
Small
https://onlinelibrary.wiley.com/doi/full/10.1002/smll.202206805
e2206805